Analyzing the synthesis route of 62266-81-3

As the paragraph descriping shows that 62266-81-3 is playing an increasingly important role.

62266-81-3, 6-Chlorobenzo[d]thiazol-2(3H)-one is a thiazole compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated,62266-81-3

Reference example 13 6-chloro-3-[2-(dimethylamino)ethyl]-2-benzothiazolone (XIIe) A solution of compound (VIII) (9.28 g, 50 mmol), N,N-dimethylaminoethylchloride hydrochloride (XIe) (7.92 g, 55 mmol), and K2 CO3 (16.58 g, 120 mmol) in acetone (93 ml) was refluxed for 20 hours with stirring. After the reaction was complete, the reaction mixture was concentrated in vacuo. The residue was extracted with ethyl acetate. The layer of ethyl acetate was dried over MgSO4 and subjected to column chromatography on silica gel. From the elude eluted with ethyl acetate, compound (XIIe) (3.3 g, yield=64.3%) was obtained as an oil. IRnumax(nujol)(cm-1):1680,1168. NMR (CDCl3)delta:2.31 (6H, S), 2.59 (2H, t, J=7.2), 4.03 (2H, t, J=7.2), 7.01(1H,d,J=8.6),7.29(1H,d,d,J=8.6,2.2),7.41(1H,d,J=2.2).

As the paragraph descriping shows that 62266-81-3 is playing an increasingly important role.

Reference£º
Patent; Shionogi & Co., Ltd.; US5473066; (1995); A;,
Thiazole | C3H3NS – PubChem
Thiazole | chemical compound | Britannica