15864-32-1, 2-Amino-6-bromobenzothiazole is a thiazole compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
6-Bromobenzo[d]thiazol-2-amine (2.3 g, 10.0 mmol) was suspended in dichloromethane (30 ml), and then 4-dimethylaminopyridine (1.3 g, 11.5 mmol) was added. The mixture was cooled in an ice-water bath under nitrogen, and acetic anhydride (1.0 ml, 11.5 mmol) was added. The resulting mixture was allowed to slowly warm to room temperature while being stirred overnight under nitrogen. Then hydrochloric acid (10%, 10 ml) was added and 5b (2.3 g, 85%) was obtained by filtration as white solid. Mp: 217.0-218.0 C; 1H NMR (DMSO-d6): delta 12.46 (s, 1H, NH), 8.24 (s, 1H, Ar-H), 7.67 (d, J = 7.2 Hz, 1H, Ar-H), 7.57 (d, J = 6.8 Hz, 1H, Ar-H), 2.21 (s, 3H, CH3). ESI-HRMS m/z: calcd for C9H7BrN2NaOS [M+Na]+: 292.9360; found 292.9360., 15864-32-1
The synthetic route of 15864-32-1 has been constantly updated, and we look forward to future research findings.
Reference：
Article; Li, Huan; Wang, Xiao-Meng; Wang, Juan; Shao, Teng; Li, Yi-Ping; Mei, Qi-Bing; Lu, She-Min; Zhang, San-Qi; Bioorganic and Medicinal Chemistry; vol. 22; 14; (2014); p. 3739 – 3748;,
Thiazole | C3H3NS – PubChem
Thiazole | chemical compound | Britannica