2941-58-4, 2-Bromo-6-methoxybenzothiazole is a thiazole compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
In an 8 mL screw cap vial was added a solution of 3-benzyl-6-mercapto-5- [METHYL-LH-PYRIMIDINE-2,] 4-dione, (0.025 g, 0.1 mmol) in dimethylformamide (1 [ML),] a solution of 2-bromo-6-methoxybenzothiazole (0.15 mmol) in dimethylformamide (0.3 mL) and diisopropylethylamine (0.05 mL, 0.3 mmol). The vial was capped and the reaction mixture was shaken for 24 hours at [100C.] The solvent was removed under vacuum. Purification was carried out via reverse- phase HPLC (ODS AC-18, [5] [T,] 30 mm [X100] mm, 3% n-propanol in acetonitrile and [3%] n-propanol in water 10 % to [90%] over 10 minutes) to give 3-benzyl-6- (6- [METHOXY-BENZOTHIAZOL-2-YLAMINO)-5-METHYL-1H-PYRIMIDINE-2,] 4-dione. MS [(APCI),] m/z [( [M+H] +)] 395.1.
2941-58-4, The synthetic route of 2941-58-4 has been constantly updated, and we look forward to future research findings.
Reference：
Patent; WARNER-LAMBERT COMPANY LLC; WO2004/14868; (2004); A2;,
Thiazole | C3H3NS – PubChem
Thiazole | chemical compound | Britannica