The synthetic route of 3622-35-3 has been constantly updated, and we look forward to future research findings.
3622-35-3, Benzo[d]thiazole-6-carboxylic acid is a thiazole compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
Reference Production Example 10 To a mixture of 11 g of benzothiazole-6-carboxylic acid, 15 g of 3-hydroxybenzylamine hydrobromide, 20 ml of pyridine and 150 ml of DMF was added 14 g of WSC at 0C, and the mixture was stirred at room temperature for 1 hour. To the reaction mixture was added water, and the solvent was distilled off under reduced pressure. To the residue was added water, and the generated solid was collected by filtration. The solid was washed with water and hexane, and dried under reduced pressure. Sixteen g ofN- (3-hydroxyphenyl) methyl-benzothiazole-6-carboxamide was obtained.N- ( 3-hydroxyphenyl )methyl-benzothiazole-6-carboxamid 1H-NMR (DMSO-d6) delta: 4.45 (2H, d, J = 5.9 Hz), 6.64 (IH, dd, J = 7.2, 1.6 Hz), 6.76-6.77 (2H, m) , 7.12 (IH, t, J = 8.0 Hz), 8.06 (IH, dd, J = 8.5, 1.7 Hz) , 8.17 (IH, d, J = 8.5 Hz) , 8.71 (IH, d, J = 1.7 Hz), 9.15 (IH, t, J = 5.9 Hz), 9.33 (IH, s) , 9.54 (IH, s) ., 3622-35-3
The synthetic route of 3622-35-3 has been constantly updated, and we look forward to future research findings.
Reference：
Patent; SUMITOMO CHEMICAL COMPANY, LIMITED; WO2009/157528; (2009); A1;,
Thiazole | C3H3NS – PubChem
Thiazole | chemical compound | Britannica