14779-17-0, 2-Amino-5-methylbenzothiazole is a thiazole compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
A benzene solution of hepta-O-benzo- b-D-lactosylisocyanate (0.001 mol, 1.1g) in 10 ml was mixed withsuspension of 2-amino benzothiazole (0.001 mol,0.15g) in 5 ml and mixture was refluxed over waterbath for 6 hr. Benzene was distilled off and stickymass obtained as a residue was triturated severaltimes with petroleum ether (60-800) to afford a whitesolid. It was crystallized from eq. ethanol.This reaction of 1-hepta-O-benzoyl- b-D-lactosylisocyanate was also extended to several other 2-aminobenzothiazoles and the corresponding 1-hepta-Obenzoyl- b-D-lactosyl-3-(2) benzothiazolyl carbamides(3b-f) have been isolated.3a: IR (KBr): 3449 (-N-H stretch), 3061 (Ar C-H),(Ar C=C), 1269 (C-N), 1174 (C-O), 1101 & 1026(Characteristic of Lactose), 852 (C-S); 1H NMR(CDCl3): 8.16-7.17 (39H, m, ArH), 6.18 (1H, s, NH),6.01 (1H, s, NH), 5.74-4.21 (14H, m, lactosyl protons);Mass : m/z 1245 (M+), 1053, 947, 931, 917, 135,121, 105., 14779-17-0
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Reference：
Article; Pande, Kedar P.; Ghayalkar, Renu B.; Indian Journal of Heterocyclic Chemistry; vol. 25; 1; (2015); p. 45 – 46;,
Thiazole | C3H3NS – PubChem
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