Some tips on 2786-51-8

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2786-51-8, 5-Chlorobenzo[d]thiazole is a thiazole compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated,2786-51-8

General procedure: A mixture of benzothiazole 1a (67.5 mg, 0.5 mmol), cyclohexane-1,3-dione 2b (112 mg, 1 mmol), KH2PO4 (136 mg, 1 mmol), DMSO (2 mL) and water (2 mL) were placed into a 15 mL flask under air. The reaction mixture was stirred in oil bath for 3 days at 80 C. The progress of the reaction was monitored by TLC. When the reaction was complete, it was neutralised with a saturated KHCO3 aqueous solution, and extracted with ethyl acetate (3 ¡Á10 mL). The extract was washed with water (3 ¡Á 5 mL) and dried over anhydrous Na2SO4. After drying, it was concentrated under reduced pressure to give the crude product, which was further purified by silica-gel column chromatography to afford 2,3-dihydro-10H-phenothiazin-4 (1H)-ones 3b (93.2 mg, yield: 86%).

As the paragraph descriping shows that 2786-51-8 is playing an increasingly important role.

Reference£º
Article; Suliman, Ayman Mohammed Yousif; Li, Yanjun; Zhang, Shaonan; Yuan, Yu; Journal of Chemical Research; vol. 39; 11; (2015); p. 657 – 660;,
Thiazole | C3H3NS – PubChem
Thiazole | chemical compound | Britannica