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Cross-coupling hydrogen evolution by visible light photocatalysis toward C(sp2)-P formation: Metal-free C-H functionalization of thiazole derivatives with diarylphosphine oxides
Visible light along with 5 mol % eosin B catalyzed the first direct C-H phosphorylation of thiazole derivatives with diarylphosphine oxides by a photoredox process in the absence of an external oxidant. The scope of thiazoles and phosphine oxides was further investigated, as was functional group tolerance. The general and operational simplicity provides a novel metal and oxidant-free alternative for the formation of heteroaryl-P bonds, and only molecular hydrogen is generated as a byproduct.
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Reference：
Thiazole | C3H8261NS – PubChem,
Thiazole | chemical compound | Britannica