Analyzing the synthesis route of 15864-32-1

15864-32-1 2-Amino-6-bromobenzothiazole 85149, athiazole compound, is more and more widely used in various fields.

15864-32-1, 2-Amino-6-bromobenzothiazole is a thiazole compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated

Step 1: Preparation of n-(6-Bromo-benzothiazol-2-yl)-acetamide A mixture of 6-bromo-benzothiazol-2-ylamine (3.0 g, 13 mmol), Ac2O (1.6 g, 16.5 mmol) and DMAP (2.4 g, 19.5 mmol) in CH2Cl2 (50 mL) was stirred at room temperature for 1 hr. Then the mixture was washed with HCl (2M), saturated Na2CO3, then brine and dried over Na2SO4. The CH2Cl2 phase was evaporated to give n-(6-Bromo-benzothiazol-2-yl)-acetamide (2.5 g, yield 71%) as a white solid., 15864-32-1

15864-32-1 2-Amino-6-bromobenzothiazole 85149, athiazole compound, is more and more widely used in various fields.

Reference：
Patent; Heald, Robert; Price, Stephen; Safina, Brian; Savy, Pascal Pierre Alexandre; Seward, Eileen Mary; Sutherlin, Daniel P.; Waszkowycz, Bohdan; US2012/202785; (2012); A1;,
Thiazole | C3H3NS – PubChem
Thiazole | chemical compound | Britannica