Downstream synthetic route of 2346-00-1

The synthetic route of 2346-00-1 has been constantly updated, and we look forward to future research findings.

2346-00-1, 2-Methyl-4,5-dihydrothiazole is a thiazole compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated

Example 2 3-Methyl-2- [(3-methyl-2-thiazolidinylidene)-methyl]-5-phenylbenzoxazolium iodide A mixture of 2-(methylthio)-5-phenylbenzoxazole (14.5 g), 4,5-dihydro-2-methylthiazole (4.75 g), and methyl p-toluenesulphonate (28.0 g) was heated at 140C for four hours. Pyridine (50 ml) was added, and the mixture was refluxed for 40 minutes. The resulting solution was cooled and treated with water (100 ml), and the solid which separated was filtered off. The filtrate was treated with sodium iodide (30 g) and concentrated hydrochloric acid (50 ml). The precipitate was filtered off, washed with water, dried, warmed with toluene, and refiltered; it was finally crystallized from methanol to yield the product as pale yellow crystals, m.p. 262 – 264 C., 2346-00-1

The synthetic route of 2346-00-1 has been constantly updated, and we look forward to future research findings.

Reference:
Patent; ILFORD Limited; EP324717; (1989); A1;,
Thiazole | C3H3NS – PubChem
Thiazole | chemical compound | Britannica