95-16-9, Benzo[d]thiazole is a thiazole compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
95-16-9, General procedure: To a reaction tube charged with xanthines (0.5 mmol), disulfides (0.3 mmol), Cu(OAc)2¡¤H2O (20 mg, 20 mol %), and AgOAc (1.7 mg, 2 mol %) was added 2 mL of xylene. After stirring at 145 C for 15 h under an O2 atmosphere, the reaction mixture was concentrated and purified by flash column chromatography on silica gel (dichloromethane/acetone = 20:1) to give 143.5 mg (yield: 95%) of compound 3aa as a white solid, mp: 147-149 C; 1H NMR (CDCl3, 600 MHz): delta 7.29-7.37 (m, 5H), 3.93 (s, 3H), 3.57 (s, 3H), 3.40 (s, 3H); 13C NMR (150 MHz, CDCl3): delta 155.0, 151.4, 148.1, 146.4, 130.9, 130.5, 129.6, 128.3, 109.6, 33.2, 29.9, 28.0.
As the paragraph descriping shows that 95-16-9 is playing an increasingly important role.
Reference£º
Article; He, Zuying; Luo, Fang; Li, Yinglong; Zhu, Gangguo; Tetrahedron Letters; vol. 54; 44; (2013); p. 5907 – 5910;,
Thiazole | C3H3NS – PubChem
Thiazole | chemical compound | Britannica